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Upcycling spent LiFePO4 via a fluorine doping-assisted direct regeneration strategy for high-rate lithium-ion batteries

Authors: Xianggang Zhou; Dan Yang; Yonghui Wang; Yingqi Li; Shanshan Xiao; Ruiqi Yao; Xingyou Lang; Qing Jiang; Yangguang Li

DOI: 10.1007/s40843-026-4229-6Status: Verified Translated Edition
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Key Findings in This Report

• • Fluorine doping in regenerated LFP reduces Li+ diffusion energy barrier and increases Fe 3d–O 2p band separation from 3.23 eV to 3.46 eV, enhancing rate capability and structural stability. • • Direct regeneration achieves energy consumption of 9.986 MJ kg−1 and greenhouse gas emissions of 0.324 kg CO2-equivalent per kg of cell, outperforming pyrometallurgy and hydrometallurgy. • • The closed-loop cathode-to-cathode process yields a net profit of $397.15 per ton of spent LFP battery recycling, based on 2025 Chinese market prices. • • Fluorine doping suppresses Fe migration and anti-site defect formation, as confirmed by density of states analysis, contributing to prolonged cycle life.